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TUTORIAL_GUIDE_2.0
NMR-TUTORIAL
Departement für Chemie, Biochemie und Pharmazie
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TUTORIAL_GUIDE_2.0
ABOUT THIS TUTORIAL
"DEPARTURE"
ELEMENTS AND SCOPE OF THE NMR TUTORIAL
THE TUTORIAL GUIDE
NAVIGATION - FORMAT ELEMENTS - DOWNLOADABLE DATA
THE LAB REPORT
BIBLIOGRAPHY - GLOSSARY
ADDITIONAL RECOMMENDATIONS
DIFFERENT ENTRY POINTS
THE BASICS OF NMR SPECTROSCOPY IN BRIEF
THE AIMS OF NMR SPECTROSCOPY
NMR SPECTRAL FEATURES
NMR EXPERIMENTS
STRATEGY AND CLASSICAL STEPS OF AN NMR INVESTIGATION
NMR DATA PROCESSING
SOFTWARE MODULES
INTRODUCTIONARY REMARKS
TOPSPIN PROCESSING/TOPSPIN SIMULATION (NMRSIM)
OBJECTIVE
DOWNLOAD AND INSTALLATION OF TOPSPIN
REGISTRATION/LICENSE GENERATION/DOWNLOAD
INSTALLATION/LICENSE ASSIGNMENT
CONFIGURATION
DOCUMENTATION
NMR DATA PROCESSING WITH TOPSPIN 4.x
INTRODUCTION
DOWNLOAD OF NMR DATA (IBUPROFEN, MENTHYL-ANTHRANILATE)
THE FORMAT OF BRUKER NMR DATA
THE TOPSPIN INTERFACE
BASIC STEPS OF NMR DATA PROCESSING
NMR DATA PROCESSING - DIFFERENT WAYS TO GO
THE ESSENTIAL OF NMR DATA PROCESSING
NMR-SIMULATION WITH TOPSPIN 4.x (NMRSIM)
INTRODUCTION
THE OPERATIONAL PROCEDURE WITH NMRSIM
LIMITATIONS
NMRSIM FILES
FIRST STEPS WITH NMRSIM
FINAL RECOMMENDATION FOR THE TUTORIAL USER
HOW TO WORK THROUGH THE TUTORIAL
HOW TO ORGANIZE THE DESKTOP
REPRESENTATIVE 1D / 2D NMR EXPERIMENTS
1D 1H-ONE PULSE EXPERIMENT (1D 1H)
1D 1H: SCOPE OF APPLICATION
1D 1H: PULSE SEQUENCE - SPECTROSCOPIC RESULT
1D 1H: SPECTRAL WINDOW
1D 1H: RESOLUTION
1D 1H: RADIOREQUENCY PULSE PROPERTIES
1D 1H: DATA ACCUMULATION: THE SIGNAL-TO-NOISE RATIO / QUANTITATION
1D 1H: THE ONE-PULSE EXPERIMENT ZG WITH OTHER NUCLEI
1D 1H: OWN EXPERIMENTAL INVESTIGATIONS
1D 1H: THE EXEMPLARY APPLICATION OF THE EXPERIMENT
1D 13C-ONE PULSE EXPERIMENT (1D 13C)
1D 13C: SCOPE OF APPLICATION
1D 13C: PULSE SEQUENCE - SPECTROSCOPIC RESULT
1D 13C: SPECTRAL WINDOW
1D 13C: RESOLUTION
1D 13C: RADIOREQUENCY PULSE PROPERTIES
1D 13C: DATA ACCUMULATION: THE SIGNAL-TO-NOISE RATIO / QUANTITATION
1D 13C: THE ONE-PULSE EXPERIMENT ZGPG WITH OTHER NUCLEI
1D 13C: OWN EXPERIMENTAL INVESTIGATIONS
1D 13C: THE EXEMPLARY APPLICATION OF THE EXPERIMENT
1D 13C-APT EXPERIMENT (1D 13C APT)
1D 13C APT: SCOPE OF APPLICATION
1D 13C APT: PULSE SEQUENCE - SPECTROSCOPIC RESULT
1D 13C APT: SPECTRAL WINDOW
1D 13C APT: RESOLUTION
1D 13C APT: RADIOFREQUENCY PULSE PROPERTIES
1D 13C APT: 13C-MULTIPLICITY DISCRIMINATION
1D 13C APT: DATA ACCUMULATION: THE SIGNAL-TO-NOISE RATIO / QUANTITATION
1D 13C APT: VARIANTS OF THE APT PULSE SEQUENCE AND RELATED EXPERIMENTS
1D 13C APT: THE APT EXPERIMENT WITH OTHER NUCLEI
1D 13C APT: OWN EXPERIMENTAL INVESTIGATIONS
1D 13C APT: THE EXEMPLARY APPLICATION OF THE EXPERIMENT
1D 13-DEPT EXPERIMENT (1D 13C DEPT)
1D 13C DEPT: SCOPE OF APPLICATION
1D 13C DEPT: PULSE SEQUENCE - SPECTROSCOPIC RESULT
1D 13C DEPT: SPECTRAL WINDOW
1D 13C DEPT: RESOLUTION
1D 13C DEPT: RADIOFREQUENCY PULSE PROPERTIES
1D 13C DEPT: 13C-MULTIPLICITY DISCRIMINATION
1D 13C DEPT: THE INFLUENCE OF THE INTER-PULSE DELAY D2
1D 13C DEPT: DATA ACCUMULATION: THE SIGNAL-TO-NOISE RATIO
1D 13C DEPT: VARIANTS OF THE DEPT PULSE SEQUENCE AND RELATED EXPERIMENTS
1D 13C DEPT: THE DEPT EXPERIMENT WITH OTHER NUCLEI
1D 13C DEPT: OWN EXPERIMENTAL INVESTIGATIONS
1D 13C DEPT: THE EXEMPLARY APPLICATION OF THE EXPERIMENT
1D 1H-COSY EXPERIMENT (1D 1H COSY)
1D 1H COSY: SCOPE OF APPLICATION
1D 1H COSY: PULSE SEQUENCE - SPECTROSCOPIC RESULT
1D 1H COSY: SPECTRAL WINDOW
1D 1H COSY: RESOLUTION
1D 1H COSY: RADIOFREQUENCY PULSE PROPERTIES
1D 1H COSY: THE INFLUENCE OF THE J-EVOLUTION DELAY D14
1D 1H COSY: SELECTIVITY WITH THE 1D COSY EXPERIMENT
1D 1H COSY: DATA ACCUMULATION - THE SIGNAL-TO-NOISE RATIO
1D 1H COSY: VARIANTS OF THE 1D COSY PULSE SEQUENCE AND RELATED EXPERIMENTS
1D 1H COSY: THE 1D COSY EXPERIMENT WITH OTHER NUCLEI
1D 1H COSY: OWN EXPERIMENTAL INVESTIGATIONS
1D 1H COSY: THE EXEMPLARY APPLICATION OF THE EXPERIMENT
2D 1H,1H-COSY EXPERIMENT (2D 1H,1H COSY)
2D 1H,1H COSY: INTRODUCTION TO 2D NMR SPECTROSCOPY
2D 1H,1H COSY: SCOPE OF APPLICATION
2D 1H,1H COSY: PULSE SEQUENCE - SPECTROSCOPIC RESULT
2D 1H,1H COSY: SPECTRAL WINDOW
2D 1H,1H COSY: RESOLUTION
2D 1H,1H COSY: THE EVOLUTION OF CROSS- AND DIAGONAL PEAKS IN BOTH TIME DOMAINS
2D 1H,1H COSY: RADIOFREQUENCY PULSE PROPERTIES
2D 1H,1H COSY: INFLUENCE OF PULSE P0
2D 1H,1H COSY: DATA ACCUMULATION - THE SIGNAL-TO-NOISE RATIO
2D 1H,1H COSY: VARIANTS OF THE 2D COSY SEQUENCE AND RELATED EXPERIMENTS
2D 1H,1H COSY: THE COSY EXPERIMENT WITH OTHER NUCLEI
2D 1H,1H COSY: OWN EXPERIMENTAL INVESTIGATIONS
2D 1H,1H COSY: THE EXEMPLARY APPLICATION OF THE EXPERIMENT
2D 1H,13C-HSQC EXPERIMENT (2D 1H,13C HSQC)
2D 1H,13C HSQC: INTRODUCTORY REMARKS
2D 1H,13C HSQC: SCOPE OF APPLICATION
2D 1H,13C HSQC: PULSE SEQUENCE - SPECTROSCOPIC RESULT
2D 1H,13C HSQC: SPECTRAL WINDOW
2D 1H,13C HSQC: RESOLUTION
2D 1H,13C HSQC: THE EVOLUTION OF CROSS- AND DIAGONAL PEAKS IN BOTH TIME DOMAINS
2D 1H,13C HSQC: RADIOFREQUENCY PULSE PROPERTIES
2D 1H,13C HSQC: THE INFLUENCE OF DELAY D4
2D 1H,13C HSQC: DATA ACCUMULATION - THE SIGNAL-TO-NOISE RATIO
2D 1H,13C HSQC: VARIANTS OF THE 2D HSQC SEQUENCE AND RELATED EXPERIMENTS
2D 1H,13C-HSQC: THE 2D HSQC EXPERIMENT WITH OTHER NUCLEI
2D 1H,13C-HSQC: A FINAL CHALLENGE - THE 2D ASAP-HSQC EXPERIMENT
2D 1H,13C HSQC: OWN EXPERIMENTAL INVESTIGATIONS
2D 1H,13C HSQC: THE EXEMPLARY APPLICATION OF THE EXPERIMENT
ARRIVAL
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Departement für Chemie, Biochemie und Pharmazie
NMR-TUTORIAL
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ELEMENTS AND SCOPE OF THE NMR TUTORIAL
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"DEPARTURE"
TUTORIAL GUIDE
Enjoy your flight over the exciting "NMR landscape" . . .
Let yourself be fascinated by the physics of NMR . . .
VERSION 2.0
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ELEMENTS AND SCOPE OF THE NMR TUTORIAL
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